专利摘要:
The system to make walls for catalytic baskets for heterogeneous synthesis reactors, particularly the distribution walls which are inserted in axial reactors in order to modify them into substantially radial (or axial-radial) reactors with low energy consumptions, consists in dividing the distribution walls (DW) into n sections, and by attaching each section end to a device consisting of two flange elements (1, 2), the radially longer one protruding over the distribution wall achieving the truing and stiffening of the entire device, the other one extending slightly into the inside of the catalytic bed. Between the internal walls of the basket (Si/CN) and the perforated distribution sheet (DW) an airspace (I) is formed by using separating rods (DI) or, in their absence, using a perforated bridge plate (LFP) as the distribution wall.
公开号:SU1611208A3
申请号:SU874203400
申请日:1987-09-24
公开日:1990-11-30
发明作者:Зарди Умберто
申请人:Аммониа Казеле С.А. (Фирма);Зарди Умберто;
IPC主号:
专利说明:

The invention relates to a catalytic basket design for heterogeneous synthesis reactors.
The aim of the invention is to increase reliability.
FIG. 1 shows a schematic representation of the proposed basket, a longitudinal partial section; in fig. 2 is a section A-A in FIG. one; Fig 3 - the node I in Fig about 2; fig 4 is the same, (airspace creation option); in Figs 5 - part of the perforated bridge wall; FIG. 6 shows a section BB in FIG. five"
The reactor comprises: housing 1, cartridge 2, a plurality of catalytic layers 3 C increasing in height from the upper to the lower layer, a gas distribution shell; 4 with perforations
over the entire height of the layer, the inner perforated shell 5, the central tube 6 and the heat exchanger 7 with the pipe. com 8o The gas distribution shell 4 is made of separate circular W polygonal sectors 9, equipped with flange-sh 10 and 11 on two end sides, forming flange connections with flanges of neighboring sectors, and a grid 12 forming an air gap 13 with the gas distribution shell 4 due to the installation of dividing rods 14, which are welded to the gas distribution shell in the perforated bridge wall. The fixation of the entire device is carried out using a tiuiaH- connection, which is kept from the bottom 10 and 11, ss are connecting each other
05
tsD
ABOUT
oo

cm
with the other at the inner end using locking or locking means, for example with a bolt 15, and which do not have matching ends, the other End Flange 10 is longer in the radial direction than the flange 11 and is welded to the perforated plate 6
The flange 10 has a continuation of 16 and IQ can freely approach or move away from the inner surface of the housing 1 so as to compensate for thermal expansion. The flange 10 centers and tightens all the fixing device and serves as the basis for welding at the end of the mesh section 12. Flange 11 is welded to the distribution shell 4 "
The flange 11 is also welded to the other 2 nd end of the 12 сетки mesh section. The mesh 12 wall is divided into sections according to sectors 9, each section being attached at one end to the alignment or centering part 10 and 25 at the other end to the part 12c. and the corresponding sectors 9 are obtained by welding the separating rods 14 to the solid portions of the -jQ sectors 9 between the mesh holes 17, or by making the gas distribution shell in the form of a corrugated plate. Instead of a corrugated perforated plate, an additional perforated plate 18 and raised sections 19 can be inserted, fastened to the gas distribution shell 4. Between the surface of the plate 18 and the surface of sections 19 there is a dd limited gap 20o
The zones in which gaps 20 co-create are spaced apart from each other, i.e., they are not over the perforations of sectors 9, as a result of which the gas, which passes radially, travels a minimum axial distance and passes
35


through the gaps 20 and 21 in the perforation 22 of the grid 12,
The device operates as follows.
Fresh gas enters through the pipe 23, rises through the air space 13, is heated in the heat exchanger 7 with hot gas, flows through the tube 6, a small part of which penetrates into the catalytic layers open from above, and crosses the first shorter upper part at the height HJ H - in the axial direction, and most of it crosses the height AND in the radial direction.
权利要求:
Claims (1)
[1]
The reacted gas is collected in the inner zones between the tube 6 and the inner shell 5 and exits at the top of the reactor. Claim 1: Catalyst basket for heterogeneous synthesis reactors made in the form of coaxially installed perforated distribution shells with safety grids, characterized in that increase reliability, each basket shell is made of separate round or polygonal sectors, provided with flanges on both sides, forming gmi with flanges of adjacent sections torants are a flantsev joint placed in a catalyst basket, with one of the flanges of its flange joint having a free end placed outside the distribution shell
7-0 Basket according to claim 1, characterized in that the distribution shell is provided with separation elements fixed on the surface facing the grid
The basket of PP, 1 and 2, characterized in that the distribution shell is corrugated
Phage. one
2
/four
.five
20
%%%%%%
S
FIG. four
FIG. five
I
sixteen
X
6
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引用文献:
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RU2684382C2|2014-12-23|2019-04-08|Касале Са|Method of implementation of the inside walls of catalytic reactors|FR508029A|1919-03-10|1920-09-29|Paul Marie Jules Robert Camill|Method and apparatus for night and daytime landing of airplanes on the ground and on all aerial devices|
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DE972297C|1954-12-25|1959-07-02|Koppers Gmbh Heinrich|Fixing and sealing of bell bottoms in fractionation columns|
DK119652B|1964-09-11|1971-02-08|Topsoe H|Reactor for performing gas phase reactions by passing a gas mixture through a bed filled with catalyst particles.|
FR2460707B1|1979-07-13|1986-09-05|Ammonia Casale Sa|SYNTHESIS REACTOR, IN PARTICULAR FOR THE CATALYTIC SYNTHESIS OF AMMONIA AND METHANOL|
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IN165082B|1985-05-15|1989-08-12|Ammonia Casale Sa|
CH666198A5|1985-09-13|1988-07-15|Ammonia Casale Sa|REACTOR FOR CATALYTIC SYNTHESIS OF AMMONIA, METHANOL AND HIGHER ALCOHOLS.|EP0365929A3|1988-10-24|1990-07-04|Ammonia Casale S.A.|System for the optimalgas distribution in reactors and walls thereof|
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EP1442786A1|2003-01-29|2004-08-04|Methanol Casale S.A.|Pseudo isothermal radial reactor|
FR2931702B1|2008-06-02|2011-08-26|Euroslot|SYSTEM FOR EXTERNALLY RETAINING A CATALYST BED IN A RADIAL FLOW REACTOR|
US9162206B2|2013-12-05|2015-10-20|Exxonmobil Research And Engineering Company|Reactor bed component for securing rigid assemblies|
FR3036977B1|2015-06-04|2021-01-29|Hmds Process|RETAINING DEVICE FOR A CATALYST BED IN A CATALYTIC REACTOR|
DE102017208319A1|2017-05-17|2018-11-22|Thyssenkrupp Ag|Radialstromeinsatzvorrichtung for predetermining at least one radial flow path in a bed reactor and assembly method and use|
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法律状态:
优先权:
申请号 | 申请日 | 专利标题
CH383786|1986-09-25|
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