瑞典专利SE1000210A1 Method for making and treating chips

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专利摘要:
This document has described and substantiated by various experiments a procedure for the pre-production of ice and the treatment of ice with the intention of reducing energy consumption in subsequent production steps in pulp production. In this method, the ﬂ icing process is performed with an ﬂ ice cutter whose cutting means (3) at the ﬂ icing has an angle (4), between the ñ direction and the side of the cut-off member closest to the ﬂ ice (2), which is in the range 75 to 105 ° causing an axially directed compression which causes the wood to crack during ﬂ icing.
公开号:SE1000210A1
申请号:SE1000210
申请日:2010-03-05
公开日:2011-09-06
发明作者:Lisbeth Hellstroem；Per Engstrand；Torbjoern Carlberg；Per Gradin；Oejvind Gregersen
申请人:Torbjoern Carlberg；Per Engstrand；Per Gradin；Gregersen Oyvind；Lisbeth Hellstroem；
IPC主号:

专利说明:

different extent. It has been found that the stucco damage to the ice is minimized at a plunge angle of about 30 °. A drop angle close to 30 ° is therefore used in the icing process according to the prior art. This drop angle has been assumed to be the most advantageous from a computational point of view in terms of chemical masses.
A major problem in the production of pulp is that this production is very energy-intensive and that the capital costs for the process equipment are very high.
The energy consumption during the ﬂ icing of the wood raw material constitutes only a small (very small) part of the total energy consumption. In the manufacture of mechanical pulps such as thermomechanical pulp and chemical mechanical pulp, on the other hand, very large amounts of electrical energy are required, often 1000 - 3000 kWh / h. In the subsequent refining steps, the largest amount of energy is consumed in relation to the total energy consumption. In the refining steps, up to 90% of the total energy consumption is consumed in the production of pulp. With today's high energy prices and the greenhouse effect debate, there is a great need to reduce energy consumption in the production of pulp. More specifically, there is a need to reduce energy consumption in the energy-intensive refining of ice. In addition, there is a great need to be able to increase production capacity in both the production of both mechanical and chemical pulps without capital investments.
A number of methods for reducing electricity consumption in the refining step have been developed over time. For example, different types of dry treatment steps of the ice before the refining (refining steps) have been prepared. Experiments have shown that ﬂ ice pre-treatment means that the specific energy [kWh / ton] consumed in the subsequent refining is reduced through the procedure.
A number of different equipments have been developed which have compressed chopped ice with the intention of reducing energy consumption in the refining process. For example, ﬂ ice can be subjected to compressive loading in a so-called compression screw (plug screw).
The compression screws have the disadvantage that these partly constitute an extra capital cost (equipment) and that an extra element is introduced in the process. The method also differs substantially from the present method in that the compressive load is not substantially directed in the fiber direction. The energy consumption in this pre-treatment is 20 - 40 kWh / ton.
The company Andritz has also developed equipment which is marketed under the name RT Pressa ﬁ ner. With RT Pressa ﬁ ner, the ice is compressed i.a. by the action of an advanced compression screw. RT Pressa ﬁ ner, however, has the disadvantage of being an extra piece of equipment in the process. Furthermore, the product RT Press Down has the disadvantage that the compressive load of the ice does not occur only substantially in the direction. Finally, it also requires extra space and can be difficult to install in an existing facility.
The energy consumption in this pre-treatment is also 20 - 40 kWh / ton.
It is further known that the energy consumption during refining can be reduced by compressing the ice in a roll nip (between at least a first and at least a second roll).
The construction means that the ice is not substantially compressed in the direction of the ice, but that the compression of the ice takes place perpendicular to the direction. The process therefore differs greatly from the process of the present patent application.
It is also previously known to seek to reduce energy consumption when refining the ice by chemically treating the ice in a step between the icing and the refining.
For example, this procedure is described in an article by Hill, Sabourin, Aichinger, Johansson presented at IMPC Sundsvall 2009.
It has unexpectedly been found that it is possible to achieve a surprisingly large reduction in the electricity energy consumption during refining without the addition of additional devices. This can be done by using load angles in accordance with the present method. The method according to the present invention goes against the traditional and accepted knowledge in the field which states that a minimization of stucco damage on the ice is the best method of application. It has been shown that the traditional and accepted know-how is incorrect if the goal is to achieve the least maintained quality of printing paper and board properties while reducing total energy consumption. The present procedure involves a completely negligible increase in energy consumption during ﬂ icing (see Verification Test 3). Objects of the Invention The main object of the present invention is to provide a method of icing which results in a substantially reduced energy consumption for decomposing the wood into individual fibers in subsequent process steps. This is done by opening up the wood structure through the compressive loads that arise during icing. This must be achieved without significantly increasing the energy consumption during ningen icing. Another object of the present invention is to create a process for icing which is combined with at least one further process step with the intention of reducing energy consumption in at least one subsequent process step in pulp production. A further object is that impregnation of the ice is facilitated and that impregnation chemicals reach larger surfaces on which they can react. An even further object of the invention is to be able to increase production capacity without investments in subsequent process equipment.
Detailed Description of the Invention The present method will be described in more detail below with reference to the accompanying schematic drawings which, by way of example, show the presently preferred embodiments of the method.
Figure 1 illustrates the angles of a cutting member.
Figure 2 shows a schematic step included in the manufacturing process for ﬂ ice (pulp) Figure 3 defines bLa. side angle 12.
Figure 4 shows results from verification experiments 1, TMP, freeness vs specific energy.
Figure 5 shows results from verifying experiment 2, TMP and CTMP (printing paper quality), freeness vs specific energy.
Figure 6 shows results from verifying experiment 2, TMP and CTMP (printing paper quality), tensile index vs specific energy.
Figure 7 shows results from verification experiment 2, TMP and CTMP (printing paper quality), light scattering coefficient vs specific energy.
Figure 8 shows results from verification experiment 2, TMP and CTMP (printing paper quality), tensile index vs freeness.
Referring to Figure 2, there is schematically shown a process for producing and treating ice in connection with the production of pulp and the like. In the icing step 6, wood chips are chipped from a raw material in the form of logs 1 and the like. The logs have preferably been pretreated via a barking step or the like 5. In a step 7, the ice can be pretreated, for example by preheating, impregnation, basing, etc., to be refined in at least one subsequent step 8. After the refining, a number of the refined ice is processed following step 9 until the pulp or the like is completed. These steps consist of prior art techniques which are generally known to those skilled in the art to which the present invention pertains. The subsequent steps are further outside the scope of the present invention. These steps are therefore not described in more detail in this patent application.
The hug ice chop used in the ﬂ ice step consists of a previously known ﬂ ice chop with one or ﬂ your cutting means 3, 14, in which ﬂ icing takes place in accordance with the present ﬂ icing method. The present invention is applicable to both ice chippers of the type disc chopping and drum chopping as well as reducer chopping.
It has unexpectedly been found that a substantially reduced energy consumption in the subsequent refining steps is achieved if the icing process is carried out so that all the cutting means of the ice cutter have an angle 4, between ﬁ the direction and the side of the cutting means closest to the ice ie load angle of 105 ° .
Preferably, the loading angle is in the range 85 ° - 100 °.
Due to the wedge shape of the cutting member, loading angles, in the range 75 ° to 105 ° according to the present invention, will cause such high compressive stresses to occur in the direction that a significant cracking of the wood structure occurs. These compressive stresses are directed in the ﬁ direction, that is, in the direction that is most favorable. The process is hereinafter referred to as Directed Chipping (DC). The main requirement for this type of icing is the use of load angles 4, in the range 75 ° to 105 °. In the ice cutters used today, the loading angles are in most cases around 115 °.
In alternative embodiments of the present invention, an adjustment is made to the length of the ice in relation to the type of wood to be frozen (alternatively taking into account the length of the type of wood to be frozen). The optimal ﬂ ice length differs between different types of wood. The adjustment of the ﬂ ice length can take place within a large range. However, for purely practical reasons, such as for subsequent feeds in screw conveyors and the like, the adjustment of the ﬂ ice length is limited to the range of 10 mm to 40 mm. However, it is conceivable that ﬂ ice lengths other than between 10 millimeters to 40 millimeters may occur in alternative embodiments.
In an alternative embodiment of the present method, the method comprises a control of the temperature of the wood (logs) in a pre-treatment step 5 before the icing takes place.
The temperature of the logs is controlled in the range - 10 ° C to 130 ° C. The temperature of the logs can be controlled in a temperate zone or similar. The temperature can be controlled by choosing the storage method of the pulpwood. This can be stored in water of different temperatures or in a conventional way in a wood yard before barking and icing. To enable high temperature of logs before. Icing, these can, for example, be temporarily stored after barking in hot process water. Since the mechanical properties of the wood depend strongly on the temperature, the cracking that can be caused by the icing will also be affected by the temperature. Choosing a pre-treatment temperature so that optimal cracking of the ice is achieved can take place in this alternative embodiment.
In an alternative embodiment, the directed icing is combined with controlling the dry content of the wood in the range of 30 to 70%. This takes place in a pre-treatment step 5. The mechanical properties of the wood change with the dry content and the effect of the load angle on the cracking of the wood can be optimized with respect to the dry content. The dry content of the wood can be controlled and kept under control through well-designed logistics in the entire chain from felling site via intermediate storage stations to pulp mills' wood yards and feeding systems for barking and icing and by choosing storage methods eg in water or with or without irrigation during storage. To optimize the dry content so that maximum cracking of the ice is achieved can take place in this embodiment.
In an alternative embodiment, the directional icing in 6 is combined with a control of the cutting speed in the range 15 to 40 m / s. Wood is generally regarded as a viscoelastic material, which means that the effect of the load angle on the cracking of the ice can be optimized by controlling the cutting speed. This control can be done by speed control of the ice chopper motor.
With reference to Figure 3 where, among other things, the direction of the log 13 in relation to the chopping disc 10, the drive shaft 11 is defined by the side angle 12, it should be mentioned that in an alternative embodiment the directional skall is combined with a control of side angles 12 in the range 0 ° to 45 °. relation to the direction of the wood material ﬁ. The state of tension created by the load angle and which in turn affects the cracking of the wood will also depend on the side angle. In this embodiment, this voltage state can be optimized with respect to providing optimal cracking of the ice. This control can be performed by different construction of the hug ice cutter's feeding system.
In an alternative embodiment, the directed ﬂ icing is combined with water, chemical or enzyme impregnation in 7. The increased cracking of the wood which is achieved with an adequate loading angle means that liquids diffuse more easily into the wood and also increase the surface area of wood to which various liquids etc. can react. favorable with.
In mechanical pulp processes such as thermomechanical pulp and chemithermomechanical pulp, chemicals are often used in order to obtain improved fibers / pulp properties adapted for specific end products (such as advanced printing paper, cardboard, tissue and uff). These chemicals can, for example, be added in connection with the sub-process steps, bas ice base, ﬂ ice impregnation, ﬂ ice preheating in 7 or ﬂ ice refining in 8. In the manufacture of mechanical pulps you can choose to use different types of sulphite, peroxide, lye and complexing agents and more recently different types of enzymes in order to improve the properties. Together with the present invention, it is found that property improvements with chemicals of this kind are markedly improved compared to if conventional icing techniques are used.
In the case of chemical pulp processes such as sulphate and salt boiling processes, both continuous and batch boiling occur. Here, the chemical impregnation is markedly improved and the cooking time can be shortened when using the invention described here. This also means that the production capacity in existing cokeries can be increased.
In the detailed description of the present invention, construction details and methods may be omitted which will be apparent to one skilled in the art to which the invention pertains. Such obvious construction details are included to the extent required for a proper function of the present invention to be achieved. Although certain preferred embodiments have been described in detail, variations and modifications within the scope of the invention may be apparent to those skilled in the art to which the invention pertains, and all of these are considered to fall within the scope of the appended claims.
Experiments performed with the present method The results from experimental studies have verified that the unexpected technical effect exists. Namely, it has been verified that major stucco damage on ice has a beneficial effect on the process that produces pulp. This new knowledge goes against the accepted and traditional know-how in the industry, which did not consider large-scale stucco damage to be preferable. In the following, three experiments made with the present method for icing are reported.
Results (verification experiment 1: Thermomechanical mass) In one experiment, ﬂ ice was produced at three different load angles; 94 °, l04 ° and ll4 °, the latter corresponds to current technology, see position 4 in Figure 1. for masses produced at different energy inputs.
The nominal ﬂ ice length was 25 mm and the cutting member speed was 20 rn / s.
Figure 4 shows the CSF values on the vertical axis and the energy input in the number of kWh per tonne of dry pulp on the horizontal axis. High CSF values indicate low machining while low CSF values indicate high machining rate. Positions 15 and 16 indicate the results for the load angles 114 ° and 104 ° respectively. Positions 17 and 18 show the results for the load angle 94 ° at high and low output, respectively. If the curve for 1 14 ° is extrapolated to CSF 350 ml, an energy input of approximately 1,700 kWh / ton is obtained. Corresponding to the 94 ° curve will be about 1,300 kWh / ton, ie a difference of about 20 - 25%. In this context, this is a very large energy gain that was completely unexpected.
Results (verification experiment 2: Chemithermomechanical pulp) In a second experiment, the effect of the loading angle in the production of a thermomechanical and two different chemothermomechanical pulps was studied. Chipping was performed in the same way as above but only for the loading angles 94 ° and 14 °. All refinements were performed here in two steps, unlike verification attempts 1.
Figure 5 shows CSF values in ml on the vertical axis and the energy input in kWh per tonne of dry mass on the horizontal axis. Figures 20 and 22 in Figure 5 show the results for ice produced at the loading angle of 94 ° and which has been added to the NaHSOg chemical with the diluent directly in the refiner and refined without the addition of chemicals. In positions 19 and 21 the same thing is shown for ﬂ ice made at the load angle 1 14 °. Here, too, it can be stated, among other things, that chipping at the loading angle of 94 ° gives ice which at the same degree of machining (CSF) requires less energy input during refining than ice made at the loading angle of 114 °.
An important property of special printing paper is the tensile strength here represented by tensile index. Figure 6 shows in position 23 the tensile index for paper as a function of the energy input in the production of TMP from ﬂ ice produced at the loading angle 1 14 ° and in position 24 the same for the loading angle 94 °. In position 25, the result is shown for paper made from the pulp obtained when 94 ° ice is refined when NaHSO 3 is added with the dilution water.
Another important property of printing paper is its opacity which depends on the light scattering properties of the paper. Figure 7 shows the specific light scattering coefficient as a function of the energy input for paper as above. Positions 26, 27 and 28 correspond to positions 23, 24 and 25 in terms of load angle etc.
In papermaking, it is advantageous that the dewatering ability of the pulp is as good as possible at predetermined important functional properties such as tensile strength and opacity.
How tensile strength represented by tensile index depends on dewatering ability represented by freeness is shown in Figure 8 where positions 29 and 30 indicate ordinary TMP of ﬂ ice made at the loading angle ll4 ° and 94 ° and positions 31 and 32 indicate refining of ﬂ ice (114 ° and 94 °) at addition of NaHSO 4 with the diluent to the reactor. The pulp produced from ﬂ ice at the loading angle of 94 ° and with NaHSO2 in the dilution water obtained the best property combination for printing paper and also the lowest energy consumption.
In the manufacture of chemical thermomechanical pulp for board and hygiene products, properties such as bulk and absorption capacity are important, however, not opacity. These types of CTMP are manufactured by dosing an alkaline sulphite solution (NazSOg) into an impregnation vessel, after which the ice is preheated so that the salt has time to react before the ice reaches the ice refiner. The ability of the pulps to give high bulk depends on the proportion of whole fibers that can be obtained. This is limited by the fact that the tip content of the pulp must be kept very low. It has been shown here that CTMP produced from ﬂ ice at the load angle of 94 ° consumes significantly less electrical energy to a certain peak content compared with CTMP produced from ﬂ ice at the load angle l14 °.
In summary, it can be stated, among other things, that (Figures 6 and 7) it is possible to achieve thermomechanical and chemical thermomechanical pulp for printing paper with lower energy consumption to the same tensile index and light scattering coefficient by producing pulp refined with ice made at the loading angle of 94 °. Furthermore, it has also been found possible to produce chemithermomechanical pulp for board and hygiene products with lower energy consumption to a certain peak content from pulp refined with ice made at the loading angle of 94 °. Results (Verification experiment 3: Impact of the loading angle on the total energy consumption in the production of pulp) If the energy saved in later stages of the refining process exceeds the increased energy consumption in the icing step at the loading angle 94 ° (compared to 1 14 °), the proposed method is the present invention of significant value. To examine the energy consumption during ﬂ icing at the load angles ll4 ° and 94 °, experiments were performed as described below.
At the loading angle of 1 14 ° and nominal chip length 25 mm, the cutting disc was rotated up to 400 rpm (revolutions per minute), which corresponds to a speed of 20 m / s for the cutting member. When this speed was reached, the energy supply to the electric motor driving the chopping disc was broken and the number of strokes that the kinetic energy stored in the rotating system was sufficient was determined. This was done so that the length of wood with the cross-sectional dimensions 50 mm x 100 mm that was ﬂ before the chopping board stopped completely, was measured and divided by the nominal length of the ﬂ ice, ie 25 mm. For the load angle 114 ° the number of strokes was 134 and for 94 ° 120. Since the moment of inertia of the rotating system is known (142 kgmz), the stored kinetic energy was determined to be 1.25 105 J just before ﬂ icing started.
The energy consumption per stroke for the two load angles 114 ° and 94 °, respectively, was 0.9 kJ and 1 kJ. Assuming that dry spruce has a density of 350 kg / ms and that each cut created a volume of 0.025 x 0.05 X 0.1 = 1.24 104 m3 and thus the weight 0.4 kg, this means that 5 kWh is consumed to ﬂ ett one ton at the load angle ll4 ° while the corresponding figure becomes 6 kWh at the load angle 94 °. This is to be compared with typical values for refining which are 1,500 - 2,000 kWh / tonne of pulp.
Advantages of the Invention Using a icing method in accordance with the present invention, a number of advantages are achieved. The most obvious advantage is that a more energy efficient refining of the ice can take place when it is manufactured in accordance with the present method. This is because the icing method according to the present patent application initiates the icing a favorable crack formation in the ice between the glaciers so that they become easier to separate.
The more open ice structure also leads to the advantage that it is possible in a much better way to get chemicals such as different types of salt solutions, peroxide solutions, lye with ﬂ era and enzymes to access the reaction surfaces and thus a more efficient process and the amount of chemicals can also be reduced to certain functional properties. mass. Chip refining is also made more efficient by the fact that the base material has been able to be impregnated much more evenly and faster, which means that it thereby avoids that parts of the wood's ice cubes have not had time to react with the chemicals in the desired manner. Inefficient reaction between the chemicals and the ice leads to the formation of larger amounts of spear, in addition to the chemicals used being used less efficiently, which is a major problem in pulp production.

权利要求:
Claims (14)
[1]
Process for the production of ﬂ ice and treatment of ﬂ ice with the intention of reducing energy consumption in subsequent production steps in pulp production, characterized in that the ﬂ icing process is carried out with an ﬂ ice cutter whose cutting means (3) at the ﬂ ice have an angle y (4) between the fiber direction and the side of the cutting means closest to the ice (2), which is in the range 75 to 105 °, causing an axially directed compression which causes the wood to crack during the icing.
[2]
Method according to claim 1, characterized in that the ﬂ ice ﬂ is frozen in lengths of 10 to 40 millimeters
[3]
Method for icing according to at least one of the preceding claims, characterized in that the method comprises a pretreatment step in which a control of the temperature of the log in the range - 10 ° C to 130 ° C takes place.
[4]
Process for icing according to at least one of the preceding claims, characterized in that the process is combined with a pretreatment step in which a control of the dry content in the range 30% to 70% takes place.
[5]
Method for icing according to at least one of the preceding claims, characterized in that the method comprises a control of the cutting speed in the range 15 rn / s to 40 rn / s.
[6]
Method for icing according to at least one of the preceding claims, characterized in that the icing takes place with side angles in the range 0 ° to 45 ° in relation to the direction of the wood material.
[7]
Process for icing according to at least one of the preceding claims, characterized in that the process is combined with water, chemical or enzyme impregnation.
[8]
Method of icing according to at least one of the preceding claims, characterized in that the method is combined with pretreatment of the ice in a compression screw
[9]
Process for icing according to at least one of the preceding claims, characterized in that the process is combined with dosing of water in connection with at least one of the process steps ﬂ ice-basing, ﬂ ice-impregnation, preheating or ﬂ ice-refining. 13
[10]
Process for icing according to at least one of the preceding claims, characterized in that the process is combined with dosing of chemicals in connection with at least one of the process steps ﬂ ice-basing, ﬂ ice-impregnation, preheating or ﬂ ice-refining.
[11]
11. Process for icing according to at least one of the preceding claims, characterized in that the process is combined with dosing of enzymes in connection with at least one of the process steps ﬂ ice-basing, ﬂ ice-impregnation, preheating or ﬂ ice-refining.
[12]
Process for icing according to at least one of the preceding claims, characterized in that the process is combined with continuous boiling of chemical pulp.
[13]
Process for icing according to at least one of the preceding claims, characterized in that the process is combined with batch cooking of chemical pulp.
[14]
Method for icing according to Claim 1, characterized in that the loading angle (4) is in the range 85 ° to 100 °.

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CN200998686Y|2007-01-12|2008-01-02|上海震旦办公设备有限公司|Thin blade for kneading machine and blade set|AT516510B1|2015-02-13|2016-06-15|Christian Brandl|Device and method for producing a profiled and defined in its height wood chips|

法律状态:

优先权:

申请号 | 申请日 | 专利标题

SE1000210A|SE535557C2|2010-03-05|2010-03-05|Process for making chips|SE1000210A| SE535557C2|2010-03-05|2010-03-05|Process for making chips|

NO11750984A| NO2542392T3|2010-03-05|2011-03-02|

PCT/SE2011/000042| WO2011108967A1|2010-03-05|2011-03-02|Method for producing and processing wood chips|

EP11750984.4A| EP2542392B1|2010-03-05|2011-03-02|Method for producing and processing wood chips|

RU2012140048/13A| RU2558431C2|2010-03-05|2011-03-02|Production and processing of wood chips|

CA2792058A| CA2792058C|2010-03-05|2011-03-02|Method for producing and processing wood chips|

CN201180011701.XA| CN102781639B|2010-03-05|2011-03-02|Method for producing and processing wood chips|

US13/581,898| US20120325370A1|2010-03-05|2011-03-02|Method for producing and processing wood chips|

MYPI2012003823A| MY161220A|2010-03-05|2011-03-02|Method for producing and processing wood chips|

SG2012062345A| SG183454A1|2010-03-05|2011-03-02|Method for producing and processing wood chips|

NZ601990A| NZ601990A|2010-03-05|2011-03-02|Method for producing and processing wood chips|

BR112012022212A| BR112012022212A2|2010-03-05|2011-03-02|method for producing and treating wood chips|

AU2011221603A| AU2011221603A1|2010-03-05|2011-03-02|Method for producing and processing wood chips|

CL2012002442A| CL2012002442A1|2010-03-05|2012-09-03|Method to produce and treat wood chips with the intention of reducing the specific energy consumption, where the process is carried out with a chipper that has a chip cutting tool at an angle between 75º to 105º to cause axial compression of the chips and cause the cracking of the chips during cutting.|

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