AEROSOL GENERATING ITEM AND SYSTEM WITH MULTIMATERIAL SUSCEPTOR AND ITS METHOD OF USE

专利摘要:
aerosol generating article with multimaterial susceptor. an aerosol generating article (10) comprises an aerosol forming substrate (20) and a susceptor (1,4) for heating the aerosol forming substrate (20). the susceptor (1,4) comprises a first susceptor material (2.5) and a second susceptor material (3.6) having a curie temperature, the first susceptor material being disposed in intimate physical contact with the second susceptor material. the first susceptor material may also have a curing temperature, the second curing temperature being less than 500°C and less than the curing temperature of the first susceptor material, if the first susceptor material has a curing temperature. the use of such a multi-material susceptor allows the heating to be optimized and the susceptor temperature to be controlled to approximate the second curie temperature without the need for direct temperature monitoring.
公开号:BR112016023589B1
申请号:R112016023589-4
申请日:2015-05-21
公开日:2021-08-24
发明作者:Oleg Mironov；Ihar Nikolaevich Zinovik；Oleg FURSA
申请人:Philip Morris Products S.A.；
IPC主号:

专利说明:

[001] This descriptive report refers to an aerosol generating article comprising an aerosol-forming substrate for generating an inhalable aerosol when heated. The aerosol-generating article comprises a susceptor for heating the aerosol-forming substrate, so that heating of the aerosol-forming substrate can be effected in a non-contact manner by induction heating. The susceptor comprises at least two different materials with different Curie temperatures. The specification also relates to a system comprising such an aerosol generating article and an aerosol generating device having an inductor for heating the aerosol generating device.
[002] Various aerosol generating articles or smoking articles in which tobacco is heated rather than combusted have been proposed in the art. One objective of such heated aerosol generating articles is to reduce known harmful smoke constituents of the type produced by the combustion and pyrolytic degradation of tobacco in conventional cigarettes.
Typically, in such heated aerosol generating articles, an aerosol is generated by transferring heat from a heat source to a physically separate substrate or aerosol forming material. During consumption, volatile compounds are released from the aerosol-forming substrate by heat transfer from the heat source and entrained in the inhaled air through the aerosol generating article. As the released compounds cool, they condense to form an aerosol that is inhaled by the user.
[004] A number of art documents disclose aerosol generating devices for consuming or smoking heated aerosol generating articles. Such devices include, for example, electrically heated aerosol generating devices in which an aerosol is generated by transferring heat from one or more electrical heating elements of the aerosol generating device to the aerosol forming substrate of a heated aerosol generating article. One advantage of such electric smoking systems is that they significantly reduce secondary smoke flow, while allowing the user to selectively suspend and resume smoking.
[005] An example of an aerosol generating article in the form of an electrically heated cigarette for use in an electrically operated aerosol generating system is disclosed in US Patent 2005/0172976 A1. The aerosol generating article is constructed to be inserted into a cigarette receiver of an aerosol generating device of the aerosol generating system. The aerosol generating device includes a power source that supplies power to a heater fixture including a plurality of electrically resistive heating elements, which are arranged to slidably receive the aerosol generating article so that the heating elements are positioned thereon. side of the aerosol generating article.
[006] The system disclosed in US Patent 2005/0172976 A1 uses an aerosol generating device comprising a plurality of external heating elements. Aerosol generating devices with internal heating elements are also known. In use, the internal heating elements of such aerosol generating devices are inserted into the aerosol forming substrate of a heated aerosol generating article such that the internal heating elements are in direct contact with the aerosol forming substrate.
[007] Direct contact between an internal heating element of an aerosol generating device and the aerosol forming substrate of an aerosol generating article can provide an efficient means for heating the aerosol forming substrate to form an inhalable aerosol. In this type of configuration, heat from the internal heating element can be transported almost instantaneously to at least a portion of the aerosol-forming substrate when the internal heating element is actuated, and this can facilitate rapid aerosol generation. Furthermore, the total heating energy required to generate an aerosol may be less than would be the case for an aerosol generating system comprising an external heating element, where the aerosol forming substrate does not directly contact the heating element external and initial heating of the aerosol-forming substrate occurs mainly by convection or radiation. Where an internal heating element of an aerosol generating device is in direct contact with an aerosol forming substrate, initial heating of portions of the aerosol forming substrate that are in direct contact with the internal heating element will be effected primarily by conduction.
[008] A system involving an aerosol generating device with an internal heating element is disclosed in WO2013102614. In this system, where a heating element is brought into contact with an aerosol-forming substrate, the heating element undergoes a thermal cycle during which it is heated and then cooled. During contact between the heating element and the aerosol-forming substrate, particles of the aerosol-forming substrate may adhere to a surface of the heating element. In addition, volatile compounds and aerosol evolved by heat from the heating element can become deposited on a surface of the heating element. Particles and compounds adhered to and deposited on the heating element can prevent the heating element from functioning optimally. These particles and compounds can also break down during use of the aerosol generating device and impart unpleasant or bitter tastes to a user. For these reasons, it is desirable to periodically clean the heating element. A cleaning process may involve the use of a cleaning tool such as a brush. If cleaning is carried out improperly, heating element may become damaged or broken. In addition, improper or reckless insertion and removal of an aerosol generating article into the aerosol generating device can also damage or break the heating element.
[009] Prior art aerosol delivery systems are known, comprising an aerosol forming substrate and an inductive heating device. The inductive heating device comprises an induction source, which produces an alternating electromagnetic field, which induces a heat-generating eddy current in a susceptor material. The susceptor material is in thermal proximity to the aerosol-forming substrate. The heated susceptor material in turn heats the aerosol-forming substrate which comprises a material that is capable of releasing volatile compounds that can form an aerosol. An example of this type of system is disclosed in WO 95/27411. A number of modalities for aerosol-forming substrates have been described in the art, which are provided in various configurations for the susceptor material in order to determine proper heating of the aerosol-forming substrate. Thus, an operating temperature of the aerosol forming substrate is sought at which the release of volatile compounds that can form an aerosol is satisfactory. It would be desirable to be able to control the operating temperature of the aerosol forming substrate in an efficient manner. As inductive heating of the aerosol forming substrate using a susceptor is a form of "non-contact heating", there is no direct means to measure the temperature inside the consumable aerosol forming substrate itself - that is, there is no contact between the device and the interior of the consumable, where the aerosol-forming substrate is.
[0010] An aerosol generating article is provided comprising an aerosol forming substrate and a susceptor for heating the aerosol forming substrate. The susceptor comprises a first susceptor material and a second susceptor material, the first susceptor material being disposed in intimate physical contact with the second susceptor material. The second susceptor material preferably has a Curie temperature that is less than 500°C. The first susceptor material is preferably used primarily to heat the susceptor when the susceptor is placed in a fluctuating electromagnetic field. Any suitable material can be used. For example, the first susceptor material can be aluminum or it can be a ferrous material such as stainless steel. The second susceptor material is preferably used primarily to indicate when the susceptor has reached a specific temperature, this temperature being the Curie temperature of the second susceptor material. The Curie temperature of the second susceptor material can be used to regulate the temperature of the entire susceptor during operation. Thus, the Curie temperature of the second susceptor material must be below the flash point of the aerosol-forming substrate. Suitable materials for the second susceptor material may include nickel and some nickel alloys.
[0011] Preferably, the susceptor may include a first susceptor material having a first Curie temperature and a second susceptor material having a second Curie temperature, the first susceptor material being disposed in intimate physical contact with the second susceptor material. The second Curie temperature is preferably lower than the first Curie temperature. As used herein, the term "second Curie temperature" refers to the Curie temperature of the second susceptor material.
[0012] By providing a susceptor having at least a first and a second susceptor material, with the second susceptor material having a Curie temperature and the first susceptor material not having a Curie temperature, or the first and second susceptor materials having the first and second Curie temperatures distinct from each other, the heating of the aerosol forming substrate and the temperature control of the heating can be separated. While the first susceptor material can be optimized with regard to heat loss and therefore heating efficiency, the second susceptor material can be optimized with regard to temperature control. The second susceptor material need not have any pronounced heating characteristics. The second susceptor material can be selected to have either a Curie temperature or a second Curie temperature, which corresponds to a preset maximum heating temperature of the first susceptor material. The desired maximum heating temperature can be set so that an overheating or burning of the aerosol formed substrate is avoided. The susceptor comprising the first and second susceptor material has a unitary structure and may be termed a bi-material susceptor or a multi-material susceptor. The close proximity of the first and second susceptor material can be advantageous in providing precise temperature control.
[0013] The first susceptor material is preferably a magnetic material with a Curie temperature above 500°C. It is desirable from a heating efficiency standpoint that the Curie temperature of the first susceptor material be above any maximum temperature that the susceptor should be capable of being heated. The second Curie temperature can preferably be selected to be less than 400°C, preferably less than 380°C or less than 360°C. It is preferable that the second susceptor material is a magnetic material selected to have a second Curie temperature that is substantially the same as a desired maximum heating temperature. That is, it is preferable that the second Curie temperature be approximately the same as the temperature to which the susceptor must be heated in order to generate an aerosol from the aerosol forming substrate. The second Curie temperature can, for example, be within the range of 200°C to 400°C or between 250°C and 360°C.
[0014] In one embodiment, the second Curie temperature of the second susceptor material can be selected so that upon being heated by a susceptor that is at a temperature equivalent to the second Curie temperature, an average temperature of the aerosol forming substrate does not pass 240°C. The overall mean temperature of the aerosol-forming substrate here is defined as the arithmetic mean of a series of temperature measurements in the central and peripheral regions of the aerosol-forming substrate. The presetting of a maximum for the overall average temperature of the aerosol forming substrate can be adapted to optimize an aerosol production.
[0015] In preferred embodiments, the aerosol generating article may include a plurality of elements mounted within a housing in the form of a column, having a mouth end and a distal end upstream of the mouth end, the plurality of elements including the aerosol forming substrate located at or towards the distal end of the column. Preferably, the aerosol forming substrate is a solid aerosol forming substrate. Preferably, the susceptor is an elongated susceptor, having a width of between 3 mm and 6 mm and a thickness between 10 micrometers and 200 micrometers. The susceptor is preferably located within the aerosol-forming substrate. It is particularly preferred that an elongated susceptor is positioned in a radially central position on the aerosol-forming substrate, preferably such that it extends along the longitudinal axis of the aerosol-forming substrate. The length of an elongated susceptor is preferably between 8 and 15 mm, for example between 10 mm and 14 mm, for example over 12 mm or 13 mm.
[0016] The first susceptor material is preferably selected for maximum heating efficiency. Inductive heating of a magnetic susceptor material located in a variable magnetic field occurs by a combination of resistive heating due to eddy currents induced in the susceptor and heat generated by magnetic hysteresis losses. Preferably the first susceptor material is a ferromagnetic metal with a Curie temperature greater than 400°C. Preferably the first susceptor is iron or an iron alloy such as steel or an iron nickel alloy. It may be particularly preferred that the first susceptor material is a 400 series stainless steel such as class 410 or class 420 or class 430 stainless steel.
[0017] The first susceptor material may alternatively be a suitable non-magnetic material such as aluminium. In a non-magnetic material, inductive heating occurs solely by resistive heating due to eddy currents.
[0018] The second susceptor material is preferably selected by having a detectable Curie temperature within a desired range, for example, at a specified temperature between 200°C and 400°C. The second susceptor material can also contribute to the susceptor's heating, but this property is less important than its Curie temperature. Preferably, the second susceptor material is a ferromagnetic metal such as nickel or a nickel alloy. Nickel has a Curie temperature of 354°C, which can be ideal for temperature control of heating in an aerosol generating article.
[0019] The first and second susceptor materials are in intimate contact forming a unitary susceptor. Thus, when heated, the first and second susceptor materials have the same temperature. The first susceptor material, which can be optimized for heating the aerosol-forming substrate, can have a first Curie temperature that is greater than any predefined maximum heating temperature. Once the second susceptor material has reached the second Curie temperature, the magnetic properties of the second susceptor material change. At the second Curie temperature, the temperature of the second susceptor material reversibly changes from a ferromagnetic phase to a paramagnetic phase. During inductive heating of the aerosol forming substrate, this phase shift of the second susceptor material can be detected without physical contact with the second susceptor material. Detection of the phase shift can allow control over the heating of the aerosol-forming substrate. For example, on detection of the phase shift associated with the second Curie temperature, inductive heating can be stopped automatically. Thus, an overheating of the aerosol-forming substrate can be avoided even if the first susceptor material, which is primarily responsible for heating the aerosol-forming substrate, has no Curie temperature or a first Curia temperature that is higher than the desired maximum heating temperature. After inductive heating stops, the susceptor cools down to a temperature lower than its second Curie temperature. At this point, the second susceptor material regains its ferromagnetic properties again. This phase shift can be detected without contact with the second susceptor material and inductive heating can then be activated again. Thus, the inductive heating of the aerosol-forming substrate can be controlled by a repeated activation and deactivation of the inductive heating device. This temperature control is performed by non-contact means. Furthermore, electronic circuits and components that are preferably already integrated in the inductive heating device may not need any additional electronic circuits and components.
[0020] Intimate contact between the first susceptor material and the second susceptor material may be made by any suitable means. For example, the second susceptor material can be plated, deposited, coated, clad or welded to the first susceptor material. Preferred methods include electroplating, galvanic plating and coating. It is preferable that the second susceptor material is present as a dense layer. A dense layer has a higher magnetic permeability than a porous layer, making it easier to detect slight changes in Curie temperature. If the first susceptor material is optimized for heating the substrate, it may be preferred so that there is no greater volume of the second susceptor material than is needed to provide a second detectable Curie spot.
[0021] In some embodiments, it may be preferable that the first susceptor material is in the form of an elongated strip having a width of between 3 mm and 6 mm and a thickness between 10 micrometers and 200 micrometers and that the second material susceptor is in the form of discrete fragments that are plated, deposited, or welded to the first susceptor material. For example, the first susceptor material can be an elongated strip of class 430 stainless steel or an elongated strip of aluminum and the second elongated material can be in the form of nickel chips having a thickness of between 5 micrometers and 30 micrometers deposited at intervals along the elongated strip of the first susceptor material. Fragments of the second susceptor material may have a width of between 0.5 mm and the thickness of the elongated strip. For example, the width can be between 1 mm and 4 mm or between 2 and 3 mm. Fragments of the second susceptor material may have a length between 0.5 mm and about 10 mm, preferably between 1 mm and 4 mm or between 2 mm and 3 mm.
[0022] In some embodiments, it may be preferable that the first susceptor material and the second susceptor material are collaminated in the form of an elongated strip having a width of between 3 mm and 6 mm and a thickness of between 10 micrometers and 200 micrometers. micrometers. Preferably, the first susceptor material has a greater thickness than the second susceptor material. The collamination can be formed by any suitable means. For example, a strip of the first susceptor material can be welded or diffusion bonded to a strip of the second susceptor material. Alternatively, a layer of second susceptor material can be deposited or plated onto a strip of first susceptor material.
[0023] In some embodiments, it may be preferable for the susceptor to be an elongated susceptor having a width of between 3 mm and 6 mm and a thickness of between 10 micrometers and 200 micrometers, the susceptor comprising a core of the first susceptor material encapsulated by the second susceptor material. Thus, the susceptor may comprise a strip of the first susceptor material that has been coated or plated by the second susceptor material. As an example, the susceptor may include a grade 430 stainless steel strip having a length of 12 mm, a width of 4 mm and a thickness of between 10 micrometers and 50 micrometers, for example 25 micrometers. Grade 430 stainless steel can be coated with a nickel layer of between 5 micrometers and 15 micrometers, for example 10 micrometers.
[0024] The susceptor can be configured for power dissipation of between 1 Watt and 8 Watt when used in conjunction with a specific inductor, for example between 1.5 Watt and 6 Watt. By "configured" it is understood that the susceptor may comprise a specific first susceptor material and may have specific dimensions that allow for power dissipation of between 1 Watt and 8 Watts when used in conjunction with a particular conductor that generates a variable magnetic field. of known frequency and known field strength.
[0025] The aerosol generating device may have more than one susceptor, for example, more than one elongated susceptor. Thus, heating can be effectively done on different portions of the aerosol-forming substrate.
[0026] An aerosol generating system is also provided, comprising an electrically operated aerosol generating device having an inductor for producing an alternative or variable electromagnetic field and an aerosol generating article comprising a susceptor as described and defined herein. The aerosol generating article engages with the aerosol generating device so that the changing electromagnetic field produced by the inductor induces a current in the susceptor, causing it to increase its temperature. The electrically operated aerosol generating device comprises electronic circuitry configured to detect the Curie transition of the second susceptor material. For example, electronic circuits can indirectly measure the apparent resistance (Ra) of the susceptor. The apparent strength changes in the susceptor when one of the materials undergoes a phase change associated with the Curie temperature. Ra can be measured indirectly, by measuring the direct current (DC) used to produce the changing magnetic field.
[0027] Preferably, the electronics are adapted for closed-loop control of the heating of the aerosol-forming substrate. Thus, electronic circuits will be able to turn off the variable magnetic field when it detects that the susceptor temperature has risen above the second Curie temperature. The magnetic field can be turned back on when the susceptor temperature has dropped below the second Curie temperature. Alternatively, the duty cycle of energy that drives the magnetic field can be reduced when the susceptor temperature increases above the second Curie temperature and decreased when the susceptor temperature decreases below the second Curie temperature.
Thus, the temperature of the susceptor can be maintained to be at the temperature of the second Curie temperature plus or minus 20°C for a predetermined period of time, thus allowing an aerosol to be formed without overheating the aerosol forming substrate. Preferably, the electronics provide a feedback circuit that allows the susceptor temperature to be controlled to be within plus or minus 15°C of the second Curie temperature, preferably within plus or minus 10°C of the second Curie temperature, preferably between about 5°C from the second Curie temperature.
[0029] The electrically operated aerosol generating device is preferably capable of generating a variable electromagnetic field with a magnetic field strength (H field strength) of between 1 and 5 kiloamps per meter (kA/m), preferably between 2 and 3 kA/m, for example, about 2.5 kA/m. The electrically operated aerosol generating device is preferably capable of generating a variable electromagnetic field with a frequency of between 1 and 30 MHz, for example between 1 and 10 MHz, for example between 5 and 7 MHz.
[0030] The susceptor is part of a consumable aerosol generating article and is used only once. Thus, any debris that forms on the susceptor during heating does not cause a problem in heating a subsequent aerosol generating article. The flavor of a sequence of aerosol generating articles can be more consistent due to the fact that a fresh susceptor acts to heat each article. Furthermore, cleaning of the aerosol generating device is less critical and can be achieved without damage to a heating element. In addition, the lack of a heating element that needs to penetrate an aerosol-forming substrate means that insertion and removal of an aerosol-generating article in an aerosol-generating device is less likely to cause inadvertent damage to the article or device. . The general aerosol generating system is therefore more robust.
[0031] As used in this document, the term "aerosol-forming substrate" is used to describe a substrate capable of releasing, upon heating, volatile compounds that can form an aerosol. Aerosols generated from the aerosol forming substrates in heated aerosol generating articles described herein may be visible or invisible and may include vapors (e.g. fine particles of substances that are in a gaseous state, which are normally liquid or solid at temperature environment), as well as gases and liquid droplets of condensed vapors.
[0032] As used in this document, the terms "upstream" and "downstream" are used to describe relative positions of the elements or portions of the elements of the aerosol generating article in relation to the direction in which a user brings the aerosol generating article heated during use.
[0033] The aerosol generating article is preferably in the form of a column comprising two ends: a mouth end and a proximal end, through which the aerosol exits the aerosol generating article and is delivered to a user, one end distal. During use, a user brings it into the mouth end to inhale the aerosol generated by the aerosol generating article. The mouth end is downstream from the distal end. The distal end may also be referred to as the upstream end and is upstream of the mouth end.
[0034] Preferably, the aerosol generating article is a smoking article that generates an aerosol that is directly inhalable into a user's lungs through the user's mouth. Most preferably, the aerosol generating article is a smoking article that generates a nicotine-containing aerosol that is directly inhalable into a wearer's lungs through the wearer's mouth.
[0035] As used herein, an "aerosol generating device" is used to describe a device that interacts with an aerosol forming substrate of an aerosol generating article to generate an aerosol. Preferably, the aerosol generating device is a smoking device that interacts with an aerosol forming substrate of an aerosol generating article to generate an aerosol that is directly inhalable into a user's lung through the user's mouth. The aerosol generating device may be a holder for a smoking article.
[0036] When used in this document, in relation to an aerosol generating article, the term "longitudinal" is used to describe the direction between the mouth end and the distal end of the aerosol generating article and the term "transverse" is used to describe the direction perpendicular to the longitudinal direction.
[0037] As used herein in connection with an aerosol generating article, the term "diameter" is used to describe the maximum dimension in the transverse direction of the aerosol generating article. When used herein in relation to the aerosol generating article, the term "length" is used to describe the maximum longitudinal dimension of the aerosol generating article.
[0038] As used herein, the term "susceptor" refers to a material that can convert electromagnetic energy into heat. When located within a variable electromagnetic field, eddy currents induced in the susceptor cause the susceptor to heat up. Furthermore, magnetic hysteresis losses within the susceptor cause additional heating of the susceptor. As the susceptor is in thermal contact with the aerosol-forming substrate, the aerosol-forming substrate is heated by the susceptor.
[0039] The aerosol generating article is preferably designed to engage with an electrically operated aerosol generating device comprising a heat induction source. The induction heating source or inductor generates the variable electromagnetic field for heating a susceptor located within the variable electromagnetic field. In use, the aerosol generating article engages with the aerosol generating device such that the susceptor is located in the variable electromagnetic field generated by the inductor.
[0040] The susceptor preferably has a length dimension greater than its width dimension or its thickness dimension, for example greater than twice its width dimension or its thickness dimension. Thus, the susceptor can be described as an elongated susceptor. The susceptor can be arranged substantially longitudinally within the column. This means that the length dimension of the elongated susceptor is arranged to be approximately parallel to the longitudinal direction of the rod, for example, within plus or minus 10 degrees of parallel to the longitudinal direction of the rod. In preferred embodiments, the elongated susceptor element may be positioned in a radially central position within the column, extending along the longitudinal axis of the column.
The susceptor may be in the form of a pin, column or blade comprising the first susceptor material and the second susceptor material. The susceptor may have a length of about 5mm and 15mm, for example between 6mm and 12mm or between 8mm and 10mm. The susceptor can have a width of between 1 mm and 6 mm and can have a thickness of between 10 micrometers and 500 micrometers, or even more preferably between 10 and 100 micrometers. If the susceptor has a constant cross section, for example a circular cross section, it has a preferable width or diameter between 1 mm and 5 mm.
[0042] Preferred susceptors can be heated to a temperature greater than 250°C. Suitable susceptors may include a non-metallic core with a metal layer disposed on the non-metallic core, for example, metallic strips of the first and second susceptor materials formed under a surface of a ceramic core.
[0043] The susceptor may have a protective outer layer, for example, a protective ceramic layer or protective glass layer encapsulating the first and second susceptor materials. The susceptor can include a protective coating formed of glass, ceramic or an inert metal formed under a core comprising the first and second susceptor materials.
[0044] The susceptor is disposed in thermal contact with the aerosol forming substrate. Thus, when the susceptor heats up, the aerosol-forming substrate is heated and an aerosol is formed. Preferably, the susceptor is disposed in direct physical contact with the aerosol-forming substrate, for example, within the aerosol-forming substrate.
[0045] The aerosol generating article may contain a single elongated susceptor. Alternatively, the aerosol generating article may include more than one elongated susceptor.
[0046] Preferably, the aerosol-forming substrate may be a solid aerosol-forming substrate. The aerosol forming substrate can comprise solid and liquid components.
Preferably, the aerosol-forming substrate comprises nicotine. In some preferred embodiments, the aerosol-forming substrate comprises tobacco. For example, the aerosol forming material can be formed from a homogenized tobacco sheet. The aerosol forming substrate can be a column formed by collecting a sheet of homogenized tobacco.
[0048] Alternatively, or in addition, the aerosol-forming substrate may comprise a non-tobacco-containing aerosol-forming material. For example, the aerosol forming material can be formed from a sheet comprising a nicotine salt and an aerosol former.
[0049] If the aerosol-forming substrate is a solid aerosol-forming substrate, the solid aerosol-forming substrate may comprise, for example, one or more of: powder, granules, pellets, pieces, wires, strips or sheets containing one or more of: herb leaf, tobacco leaf, tobacco twig fragments, expanded tobacco, and homogenized tobacco.
[0050] Optionally, the solid aerosol forming substrate may contain volatile tobacco or non-tobacco flavoring compounds, which are released upon heating the solid aerosol forming substrate. The solid aerosol forming substrate may also contain capsules which, for example, include the additional volatile tobacco flavoring compounds or non-tobacco volatile additional flavor compounds, and these capsules may melt during heating of the solid aerosol forming substrate.
[0051] Optionally, the solid aerosol forming substrate can be provided or incorporated into a thermally stable carrier. The carrier can be in the form of powder, granules, pellets, pieces, threads, strips or sheets. The solid aerosol forming substrate may be deposited onto the surface of the carrier in the form of, for example, a sheet, foam, gel or paste. The solid aerosol forming substrate can be deposited over the entire surface of the carrier or, alternatively, it can be deposited in a pattern to provide non-uniform flavor distribution during use.
[0052] As used herein, the term "homogenized tobacco material" denotes a material formed by the agglomeration of particulate tobacco.
[0053] As used in this document, the term 'sheet' means a laminar element with a length and width substantially greater than its thickness.
[0054] As used herein, the term 'grouped' is used to describe a sheet that is twisted, folded or otherwise compressed or constricted substantially transversely to the longitudinal axis of the aerosol generating article.
[0055] In a preferred embodiment, the aerosol forming substrate comprises a grouped textured sheet of homogenized tobacco material.
[0056] As used herein, the term 'textured sheet' denotes a sheet that has been crimped, embossed, embossed, perforated or deformed. The aerosol forming substrate may comprise grouped textured sheets of homogenized tobacco material comprising a plurality of spaced indents, ridges, perforations or combinations thereof.
[0057] In a particularly preferred embodiment, the aerosol-forming substrate comprises a grouped crimped sheet of homogenized tobacco material.
[0058] The use of a textured sheet of homogenized tobacco material can advantageously facilitate grouping of the sheet of homogenized tobacco material to form an aerosol forming substrate.
[0059] As used herein, the term "crimped sheet" indicates a sheet having a plurality of substantially parallel edges or corrugations. Preferably, when the aerosol generating article has been assembled, the substantially parallel edges or corrugations will extend along or parallel to the longitudinal axis of the aerosol generating article. This favorably facilitates the collection of the crimped sheet of homogenized tobacco material to form the aerosol-forming substrate. However, it will be more appropriate that the crimped sheets of homogenized tobacco material for inclusion in the aerosol generating article may, alternatively or in addition to the above, have several basically parallel edges or corrugations arranged at an acute or obtuse angle to the longitudinal axis of the aerosol generating article when the aerosol generating article has been assembled.
The aerosol forming substrate may be in the form of a plug comprising an aerosol forming material circumscribed by a paper or other wrapping. Where an aerosol-forming substrate is in the form of a plug, the entire plug including any wraps shall be considered to be the aerosol-forming substrate.
[0061] In a preferred embodiment, the aerosol generating substrate comprises a plug comprising a grouped sheet of homogenized tobacco material or other aerosol forming material circumscribed by an envelope. Preferably, the susceptor is an elongated susceptor and the or each elongated susceptor is positioned within the plug in direct contact with the aerosol forming material.
[0062] As used herein, the term 'aerosol former' is used to describe any suitable known compound or mixture of compounds which, when in use, facilitate the formation of an aerosol and which is substantially resistant to thermal degradation at temperature of the aerosol generating article.
[0063] Suitable aerosol formers are known in the art and include, but are not limited to: polyhydric alcohols such as propylene glycol, triethylene glycol, 1,3-butanediol and glycerin; esters of polyhydric alcohols, such as glycerol mono-, di- or triacetate; and aliphatic esters of mono-, di- or polycarboxylic acids, such as dimethyl dodecanedioate and dimethyl tetradecanedioate.
Preferred aerosol formers are polyhydric alcohols or mixtures thereof, such as propylene glycol, triethylene glycol, 1,3-butanediol and, more preferably, glycerin.
[0065] The aerosol forming substrate may further comprise a single aerosol former. Alternatively, the aerosol forming substrate can comprise a combination of two or more aerosol formers.
[0066] Preferably, the aerosol former substrate has an aerosol former content greater than 5% on a dry weight basis.
[0067] The aerosol former substrate may have an aerosol former content between approximately 5% and approximately 30% based on dry weight.
[0068] In a preferred embodiment, the aerosol forming substrate has an aerosol former content of about 20% on a dry weight basis.
[0069] Aerosol forming substrates comprising bundled sheets of homogenized tobacco for use in the aerosol generating article can be produced by methods known in the art, for example the methods disclosed in WO 2012/164009 A2.
[0070] Preferably, the aerosol-forming substrate has an outer diameter of at least 5 mm. The aerosol forming substrate may have an outer diameter of between approximately 5 millimeters and approximately 12 millimeters, for example, approximately 5 millimeters and approximately 10 millimeters, or approximately 6 millimeters and approximately 8 millimeters. In a preferred embodiment, the aerosol forming substrate has an outer diameter of 7.2 mm +/- 10%.
[0071] The aerosol forming substrate may have a length of between about 5 mm and about 15 mm, for example between about 8 mm and about 12 mm. In one embodiment, the aerosol-forming substrate can have a length of approximately 10 mm. In a preferred embodiment, the aerosol forming substrate is approximately 12 mm in length. Preferably, the elongated susceptor is approximately the same length as the aerosol-forming substrate.
[0072] Preferably, the aerosol forming substrate is substantially cylindrical.
[0073] The support element may be located immediately downstream of the aerosol-forming substrate and may abut against the aerosol-forming substrate.
[0074] The support element can be formed from any suitable material or combination of materials. For example, the supporting element can be formed from one or more materials selected from the group consisting of: cellulose acetate; cardboard; crimped paper, such as heat-resistant crimped paper or crimped parchment paper; and polymeric materials such as low density polyethylene (LDPE). In a preferred embodiment, the support element is formed from cellulose acetate.
[0075] The support element may include a hollow tubular element. In a preferred embodiment, the support element comprises a hollow cellulose acetate tube.
[0076] The support element preferably has an outer diameter that is approximately equal to the outer diameter of the aerosol generating article.
[0077] The support element may have an outer diameter of between approximately 5 millimeters and approximately 12 millimeters, for example, between approximately 5 millimeters and approximately 10 millimeters or between approximately 6 millimeters and approximately 8 millimeters. In a preferred embodiment, the support element has an outer diameter of 7.2 millimeters +/- 10%.
[0078] The support element can have a length of between approximately 5 millimeters and approximately 15 mm. In a preferred embodiment, the support element is approximately 8 millimeters long.
[0079] An aerosol cooling element may be located downstream of the aerosol forming substrate, for example an aerosol cooling element may be located immediately downstream of a support element and may abut the support element.
[0080] The aerosol cooling element may be located between a support element and a mouth located at the extreme downstream end of the aerosol generating article.
[0081] The aerosol cooling element can have a total surface area of between approximately 300 square millimeters per millimeter long and approximately 1000 square millimeters per millimeter long. In a preferred embodiment, the aerosol cooling element has a total surface area of approximately 500 square millimeters per millimeter in length.
[0082] The aerosol cooling element may alternatively be called "heat exchanger".
[0083] The aerosol cooling element preferably has low drag resistance. That is, the aerosol cooling element preferably offers low resistance to the passage of air through the aerosol generating article. Preferably, the aerosol cooling element does not substantially affect the drag resistance of the aerosol generating article.
[0084] The aerosol cooling element may comprise a plurality of longitudinally extending channels. The plurality of longitudinally extending channels can be defined by a sheet material that has been crimped, pleated, grouped and/or folded to form the channels. The plurality of longitudinally extending channels can be defined by a single individual sheet that has been crimped and/or pleated and/or grouped and/or folded to form multiple channels. Alternatively, the plurality of longitudinally extending channels can be defined by multiple plates that have already been crimped and/or pleated and/or grouped and/or folded to form multiple channels.
[0085] In some embodiments, the aerosol cooling element may comprise a grouped sheet of material selected from a group consisting of sheet metal, polymeric material, and substantially non-porous paper or paperboard. In some embodiments, the aerosol cooling element may comprise an assembled sheet of material selected from a group consisting of polyethylene (PE), polypropylene (PP), polyvinylchloride (PVC), polyethylene terephthalate (PET), polylactic acid (PLA), cellulose acetate (CA), and aluminum foil.
[0086] In a preferred embodiment, the aerosol cooling element comprises a grouped sheet of biodegradable material. For example, a bundled sheet of non-porous paper or a bundled sheet of biodegradable polymeric material such as, for example, a polylactic acid or a grade of Mater-Bi® (a commercially available family of starch-based copolyesters).
[0087] In a preferred embodiment, the aerosol cooling element comprises a grouped sheet of polylactic acid.
[0088] The aerosol cooling element can be formed from a grouped sheet of material with specific surface area between about 10 millimeters per square milligram and about 100 millimeters per square milligram weight. In some embodiments, the aerosol cooling element can be formed from an assembled sheet of material having a specific surface area of about 35 mm2 /mg.
[0089] The aerosol generating article may include a mouth located at the downstream end of the aerosol generating article. The mouth is located immediately downstream of an aerosol coolant element and may abut against the aerosol coolant element. The mouth can comprise a filter. The filter can be formed from one or more suitable filtering materials. Many of these filter materials are known in the art. In one embodiment, the mouth may include a filter formed from cellulose acetate fibers.
[0090] The mouth preferably has an outer diameter that is approximately equal to the outer diameter of the aerosol generating article.
[0091] The mouth may have an outside diameter of a diameter between approximately 5 millimeters and approximately 10 millimeters, for example, between approximately 6 millimeters and approximately 8 millimeters. In a preferred embodiment, the mouth has an external diameter of 7.2 millimeters +/- 10%.
[0092] The mouth can be between approximately 5 millimeters and approximately 20 millimeters in length. In a preferred embodiment, the mouth is approximately 14 millimeters long.
[0093] The mouth can be between approximately 5 millimeters and approximately 14 millimeters in length. In a preferred embodiment, the mouth is approximately 7 millimeters long.
[0094] The elements of the aerosol-forming article, for example, the aerosol-forming substrate and any other elements of the aerosol-generating article such as a support element, an aerosol cooling element and a mouth, are circumscribed by a casing external. The outer casing can be made of any suitable material or combination of materials. Preferably, the wrapper is a cigarette paper.
[0095] The aerosol generating article may have an outer diameter of between approximately 5 millimeters and approximately 12 millimeters, for example, of between approximately 6 millimeters and approximately 8 millimeters. In a preferred embodiment, the aerosol generating article has an outside diameter of 7.2mm +/10%.
[0096] The aerosol generating article may have an overall length of between approximately 30 millimeters and approximately 100 millimeters. In preferred embodiments, the aerosol generating article has an overall length of approximately 40mm and 50mm, for example approximately 45mm.
[0097] The aerosol generating device of the aerosol generating system may include: a housing; a cavity for receiving the aerosol generating article, an inductor arranged to generate a variable electromagnetic field within the cavity; an electrical power supply connected to the inductor; and a control element configured to control the power supply from the power supply to the inductor.
[0098] In preferred embodiments the device may include a DC power source, such as a rechargeable battery, providing a DC power supply voltage and a DC current, power supply electronics comprising a DC/AC inverter to convert the DC current into an AC current to supply the inductor. The aerosol generating device may further comprise an impedance matching network between the DC/AC inverter and the inductor to improve the energy transfer efficiency between the inverter and the inductor.
[0099] The control element is preferably is coupled to, or comprises, a monitor or monitoring means to monitor the DC current supplied by the DC power source. DC current can provide an indirect indication of the apparent resistance of a susceptor located in the electromagnetic field, which in turn can provide a means of detecting a Curie transition in the susceptor.
[00100] The inductor may comprise one or more coils that generate a variable electromagnetic field. The coil or coils can surround the cavity.
[00101] Preferably, the device is capable of generating a variable electromagnetic field of between 1 and 30 MHz, for example between 2 and 10 MHz, for example between 5 and 7 MHz.
[00102] Preferably, the device is capable of generating a variable electromagnetic field with a magnetic field strength (H field strength) of between 1 and 5 kiloamps per meter (kA/m), preferably between 2 and 3 kA/m, for example, about 2.5 kA/m.
[00103] Preferably, the aerosol generating device is a portable or handheld aerosol generating device that can be held by the user between the fingers of a single hand in a comfortable manner.
[00104] The aerosol generating device may be substantially cylindrical in shape.
[00105] The aerosol generating device can have a length between approximately 70 millimeters and approximately 120 millimeters.
[00106] The power supply can be any suitable power supply, for example a DC voltage source such as a battery. In one embodiment, the power supply is a lithium-ion battery. Alternatively, the energy source can be a nickel metal hydride battery, a nickel cadmium battery or a lithium-based battery, eg lithium cobalt, lithium iron phosphate, lithium titanate or a polymer battery of lithium.
[00107] The control element can be a simple key. Alternatively, the control element can be electrical circuits and can comprise one or more microprocessors or microcontrollers.
[00108] The aerosol generating system may comprise such an aerosol generating device and one or more aerosol generating articles comprising a susceptor as described above, the aerosol generating articles being configured to be received in a cavity of the aerosol generating device so as that the susceptor located within the aerosol generating article is positioned within a variable electromagnetic field generated by the inductor.
[00109] The method of using an aerosol generating article as described above may comprise the steps of positioning an article relative to an electrically operated aerosol generating device such that the elongated susceptor of the article is within a variable electromagnetic field generated by the device, the variable electromagnetic field causing the susceptor to heat up and monitoring at least one parameter of the electrically operated aerosol generating device to detect the Curie transition of the second susceptor material. For example, the DC current supplied by the power supply can be monitored to provide an indirect measure of the apparent resistance in the susceptor. The electromagnetic field can be controlled in order to keep the temperature of the susceptor to be approximately the same temperature as the Curie transition of the second susceptor material. The electromagnetic field can be turned on and off to keep the susceptor temperature within desired limits. The device duty cycle can be changed to keep the susceptor temperature within desired limits.
[00110] The electrically operated aerosol generating device may be any device described in this document. Preferably, the frequency of the varying electromagnetic field is maintained to be between 1 and 30 MHz, for example between 5 and 7 MHz.
[00111] A method of producing an aerosol generating article as described or defined herein may include the steps of assembling a plurality of elements in the form of a column having a mouth end and a distal end upstream of the end. of mouth, the plurality of elements including an aerosol-forming substrate and a susceptor, preferably an elongated susceptor element disposed substantially longitudinally disposed within the column, in thermal contact with the aerosol-forming substrate. The susceptor is preferably in direct contact with the aerosol forming substrate.
[00112] Advantageously, the aerosol-forming substrate can be produced by grouping at least one sheet of aerosol-forming material and having the circumscription of the sheet grouped by an envelope. A suitable method for producing such an aerosol forming substrate for a heated aerosol generating article is disclosed in WO2012164009. The sheet of aerosol forming material may be a homogenized tobacco sheet. Alternatively, the sheet of aerosol forming material may be a non-tobacco material, for example a sheet comprising a nicotine salt and an aerosol former.
[00113] An elongated susceptor, or each elongated susceptor, may be inserted into the aerosol-forming substrate prior to the aerosol-forming substrate being assembled with other elements to form an aerosol-generating article. Alternatively, the aerosol-forming substrate can be assembled with other elements before the susceptor is inserted into the aerosol-forming substrate.
[00114] The characteristics described in relation to an aspect or modality may also be applicable to other aspects and modalities. The specific modalities will now be described with reference to the Figures, in which:
[00115] Figure 1A is a plan view of a susceptor for use in an aerosol generating article in accordance with an embodiment of the invention;
[00116] Figure 1B is a side view of the susceptor of Figure 1A;
[00117] Figure 2A is a plan view of a second susceptor for use in an aerosol generating article according to an embodiment of the invention;
[00118] Figure 2B is a side view of the susceptor of Figure 2A;
[00119] Figure 3 is a schematic cross-sectional illustration of a specific embodiment of an aerosol generating article incorporating a susceptor, as illustrated in Figures 2A and 2B;
[00120] Figure 4 is a schematic cross-sectional illustration of a specific embodiment of an electrically operated aerosol generating device for use with the aerosol generating article illustrated in Figure 3,
[00121] Figure 5 is a schematic cross-sectional illustration of the aerosol generating article of Figure 3 engaged with the electrically operated aerosol generating device of Figure 4;
[00122] Figure 6 is a block diagram showing the electronic components of the aerosol generating device described in relation to Figure 4; and
[00123] Figure 7 is a graph of dc current vs. time illustrating the remotely detectable current changes that occur when a susceptor material undergoes a phase transition associated with its Curie point.
[00124] Inductive heating is a known phenomenon described by Faraday's law of induction and Ohm's law. More specifically, the Faraday law of induction states that if the magnetic induction in a conductor is changing, an altered electric field is produced in the conductor. Once this electric field is produced in a conductor, a current, known as an eddy current, will flow in the conductor according to Ohm's law. Eddy current will generate heat proportional to current density and conductor resistivity. A conductor that is capable of being inductively heated is known as a susceptor material. The present invention employs an inductive heating device equipped with an inductive heating source, such as an induction coil, which is capable of generating an alternating electromagnetic field from an AC source such as an LC circuit. Heat-generating eddy currents are produced in susceptor material that is in thermal proximity to an aerosol-forming substrate that is capable of releasing volatile compounds that can form an aerosol upon heating. The primary heat transfer mechanisms from the susceptor material to the solid material are: conduction, radiation and possibly convection.
[00125] Figure 1A and Figure 1B illustrate a specific example of a unitary multimaterial susceptor for use in an aerosol generating article according to an embodiment of the invention. Susceptor 1 is in the form of an elongated strip having a length of 12 mm and a width of 4 mm. The susceptor is formed from a first susceptor material 2 which is intimately coupled to the second susceptor material 3. The first susceptor material 2 is in the form of a stainless steel class 430 strip measuring 12 mm by 4 mm by 35 micrometers. The second susceptor material 3 is a nickel fragment measuring 3 mm by 2 mm by 10 micrometers. The nickel fragment was galvanized to the stainless steel strip. Grade 430 stainless steel is a ferromagnetic material with a Curie temperature greater than 400°C. Nickel is a ferromagnetic material, with a Curie temperature of about 354°C.
[00126] In other embodiments, the material that forms the first and second susceptor materials can be varied. In other embodiments there may be more than one fragment of the second susceptor material located in intimate contact with the first susceptor material.
[00127] Figure 2A and Figure 2B illustrate a second specific example of a unitary multimaterial susceptor for use in an aerosol generating article according to an embodiment of the invention. Susceptor 4 is in the form of an elongated strip having a length of 12 mm and a width of 4 mm. The susceptor is formed from a first susceptor material 5 which is intimately coupled to the second susceptor material 6. The first susceptor material 5 is in the form of a stainless steel class 430 strip with dimensions 12mm by 4mm by 25 micrometers. The second susceptor material 6 is in the form of a nickel steel strip measuring 12 mm by 4 mm by 10 micrometers. The susceptor is formed by coating the nickel strip 6 to the stainless steel strip 5. The total thickness of the susceptor is 35 micrometers. Susceptor 4 of Figure 2 can be termed a two-layer or multi-layer susceptor.
[00128] Figure 3 illustrates an aerosol generating article 10 according to a preferred embodiment. The aerosol generating article 10 comprises four elements disposed in coaxial alignment: an aerosol forming substrate 20, a support element 30, an aerosol cooling element 40 and a mouth 50. Each of these four elements is a substantially cylindrical element, each having substantially the same diameter. These four elements are arranged sequentially and are circumscribed by an outer shell 60 to form a cylindrical column. An elongated bilayer susceptor 4 is located within the aerosol-forming substrate, in contact with the aerosol-forming substrate. Susceptor 4 is the susceptor described above in relation to Figure 2. Susceptor 4 has a length (12 mm) that is approximately the same as the length of the aerosol forming substrate and is located along a radially central axis of the forming substrate. aerosol spray.
[00129] The aerosol generating article 10 has a proximal or mouth end 70, which a user inserts into their mouth during use, and a distal end 80 located at the opposite end of the aerosol generating article 10 to the end of mouth 70. Once assembled, the total length of the aerosol generating article 10 is about 45 mm and the diameter is about 7.2 mm.
[00130] In use, air is drawn through the aerosol generating article by a user from the distal end 80 to the mouth end 70. The distal end 80 of the aerosol generating article may also be described as the upstream end of the aerosol generating article 10 and the mouth end 70 of the aerosol generating article 10 may also be described as the downstream end of the aerosol generating article 10. The elements of the aerosol generating article 10 located between the mouth end 70 and the distal end 80 can be described as being upstream of the mouth end 70 or, alternatively, downstream of the distal end 80.
[00131] The aerosol forming substrate 20 is located at the distal end or upstream end 80 of the aerosol generating article 10. In the embodiment illustrated in Figure 3, the aerosol forming substrate 20 comprises a grouped sheet of crimped homogenized tobacco material. circumscribed by an envelope. The crimped sheet of the homogenized tobacco material comprises glycerin as an aerosol former.
[00132] The supporting element 30 is located immediately downstream of the aerosol forming substrate 20 and abuts the aerosol forming substrate 20. In the embodiment shown in Figure 3, the supporting element is a hollow cellulose acetate tube. The support member 30 locates the aerosol forming substrate 20 at the extreme distal end 80 of the aerosol generating article. The backing member 30 also acts as a separator to separate the aerosol cooling element 40 from the aerosol generating article 10 from the aerosol forming substrate 20.
[00133] The aerosol cooling element 40 is located immediately downstream of the bearing element 30 and abutting the bearing element 30. In use, volatile substances released by the aerosol forming substrate 20 pass through the aerosol cooling element 40 toward the mouth end 70 of the aerosol generating article 10. The volatile substances may cool within the aerosol cooling element 40 to form an aerosol that is inhaled by the user. In the embodiment illustrated in Figure 3, the aerosol cooling element comprises a grouped and crimped sheet of polylactic acid circumscribed by a wrapper 90. The grouped and crimped sheet of polylactic acid defines a plurality of longitudinal channels extending along the length of the element aerosol coolant 40.
The mouth 50 is located immediately downstream of the aerosol coolant element 40 and abuts the aerosol coolant element 40. In the embodiment illustrated in Figure 3, the mouth 50 comprises a conventional low-pressure cellulose acetate fiber filter filtration efficiency.
[00135] To assemble the aerosol generating article 10, the four cylindrical elements described above are aligned and firmly enclosed within the outer wrapper 60. In the embodiment illustrated in Figure 3, the outer wrapper is a conventional cigarette paper. Susceptor 4 may be inserted into aerosol forming substrate 20 during the process used to form the aerosol forming substrate, before the plurality of elements together form a column.
[00136] The aerosol generating article 10 illustrated in Figure 3 is designed to engage with an electrically operated aerosol generating device comprising an induction coil or inductor in order to be smoked or consumed by a user.
[00137] A schematic cross-sectional illustration of an electrically operated aerosol generating device 200 is shown in Figure 4. The aerosol generating device 200 comprises an inductor 210. As shown in Figure 4, the inductor 210 is located adjacent to a distal portion 231 of a substrate receiving chamber 230 of the aerosol generating device 200. In use, the user inserts an aerosol generating article 10 into the substrate receiving chamber 230 of the aerosol generating device 200 such that the aerosol forming substrate 20 of the aerosol generating article 10 is located adjacent to the inductor 210.
[00138] The aerosol generating device 200 comprises a battery 250 and electronic components 260 that allow the inductor 210 to be actuated. Such actuation may be manually operated or may occur automatically in response to a user puffing on an aerosol generating article 10 inserted into substrate receiving chamber 230 of aerosol generating device 200. Battery 250 provides a DC current. The electronics include a DC/AC inverter to supply the inductor with high-frequency AC current.
[00139] When the device is actuated, a high-frequency alternating current is passed through coils of wire that form part of the inductor. This causes the inductor 210 to generate a variable electromagnetic field within the distal portion 231 of the substrate receiving cavity 230 of the device. The electromagnetic field preferably varies with a frequency of between 1 and 30 MHz, preferably between 2 and 10 MHz, for example between 5 and 7 MHz. When an aerosol generating article 10 is correctly situated in the substrate receiving cavity 230, the susceptor 4 of article 10 is located within this variable electromagnetic field. The variant field generates eddy currents within the susceptor, which is consequently heated. Additional heating is provided by magnetic hysteresis losses within the susceptor. The heated susceptor heats the aerosol forming substrate 20 of the aerosol generating article 10 to a temperature sufficient to form an aerosol. The aerosol is drawn downstream through the aerosol generating article 10 and inhaled by the user. Figure 5 illustrates an aerosol generating article in engagement with an electrically operated aerosol generating device.
[00140] Figure 6 is a block diagram showing the electronic components of the aerosol generating device 200 described in relation to Figure 4. The aerosol generating device 200 comprises a DC power source 250 (battery), a microcontroller (drive unit). microprocessor control) 3131, a DC/AC inverter 3132, a corresponding network 3133 for load adaptation and an inductor 210. The microprocessor control unit 3131, the CC/AC inverter 3132 and the corresponding network 3133 are part of the electronic components of the power supply 260. The DC supply voltage VDC and the DC IDC current drawn from the power supply 250 are provided by the feedback channels to the microprocessor control unit 3131 preferably by measuring both the DC supply voltage VDC and the DC current IDC taken from DC power supply 250 to control the additional AC power supply PAC to inductor 3134. A corresponding network 3133 can be r provided for better adaptation to the load, but this is not essential.
[00141] As the susceptor 4 of an aerosol generating article 10 is heated during operation, its apparent resistance (Ra) increases. This increase in resistance can be remotely detected by monitoring the DC current drawn from the DC power source 250, which at constant voltage decreases as the susceptor temperature increases. The high-frequency variable magnetic field provided by inductor 210 induces eddy currents in close proximity to the surface of the susceptor, an effect that is known as the film effect. Resistance in the susceptor depends, in part, on the electrical resistivity of the first and second susceptor materials and, in part, on the depth of the film layer in each material available for induced eddy currents. Once the second susceptor material 6 (nickel) has reached its Curie temperature, it loses its magnetic properties. This causes an increase in the film layer available for eddy currents in the second susceptor material, which causes a decrease in the apparent resistance of the susceptor. The result is a temporary increase in detected DC current when the second susceptor material reaches its Curie point. This can be seen in the graph in Figure 7.
[00142] By remote sensing the change in resistance in the susceptor, the time at which susceptor 4 reaches the second Curie temperature can be determined. At this point, the susceptor is at a known temperature (354°C in the case of a nickel susceptor). At this point, the electronics in the device operate to vary the power supplied and thereby reduce or stop heating of the susceptor. The susceptor temperature then decreases to below the Curie temperature of the second susceptor material. Power supply can be increased again, or resumed, after a period of time or after it has been detected that the second susceptor material has cooled below its Curie temperature. By using such a feedback loop, the susceptor temperature can be maintained at approximately that of the second Curie temperature.
[00143] The specific modality described in relation to Figure 3 is composed of an aerosol forming substrate formed from homogenized tobacco. In other embodiments, the aerosol-forming substrate can be formed of a different material. For example, a second specific embodiment of an aerosol-generating article has elements that are identical to those described above in relation to the embodiment of Figure 3, with the exception that the aerosol-forming substrate 20 is formed from a tobacco-free sheet or cigarette paper that has been soaked in a liquid formulation comprising nicotine pyruvate, glycerin and water. Cigarette paper absorbs the liquid formulation and the non-tobacco sheet material therefore comprises nicotine pyruvate, glycerin and water. The glycerine to nicotine ratio is 5:1. In use, the aerosol forming substrate 20 is heated to a temperature of about 220 degrees Celsius. At this temperature, an aerosol comprising nicotine pyruvate, glycerin and water is developed and can be extracted through the filter 50 and into the user's mouth. It is observed that the temperature to which substrate 20 is heated is considerably less than the temperature that would be required to develop an aerosol from a tobacco substrate. As such, it is preferable that the second susceptor material is a material with a lower Curie temperature than nickel. A suitable nickel alloy can for example be selected.
[00144] The examples of modalities described above are not intended to limit the scope of the claims. Other embodiments consistent with the examples of embodiments described above will be apparent to those skilled in the art.

权利要求:
Claims (18)
[0001]
1. An aerosol generating article (10) comprising an aerosol forming substrate (20) and a susceptor (1,4) for heating the aerosol forming substrate (20), characterized in that the susceptor (1,4) comprises a first susceptor material (2.5) and a second susceptor material (3.6), the first susceptor material being disposed in intimate physical contact with the second susceptor material and the second susceptor material having a Curie temperature that is less than 500 °C.
[0002]
2. Aerosol generating article according to claim 1, characterized in that the first susceptor material is aluminum, iron or an iron alloy, for example a stainless steel of class 410, 420 or 430 and the second susceptor material is nickel or a nickel alloy.
[0003]
3. An aerosol generating article according to claim 1 or 2, characterized in that the susceptor (1.4) comprises the first susceptor material (2.5) with a first Curie temperature and the second susceptor material ( 3.6) having a second Curie temperature that is less than 500°C, the second Curie temperature being lower than the first Curie temperature.
[0004]
4. An aerosol generator article, according to any one of the preceding claims, characterized in that the Curie temperature of the second susceptor material is less than 400°C.
[0005]
5. An aerosol generating article (10) according to any one of the preceding claims, characterized in that it comprises a plurality of elements mounted within a housing in the form of a column with a mouth end (70) and a distal end (80) downstream of the mouth end, the plurality of elements including the aerosol-forming substrate (20) located at or towards the distal end of the column, in which the aerosol-forming substrate is a solid aerosol-forming substrate and the susceptor is an elongated susceptor with a width of between 3 mm and 6 mm and a thickness between 10 micrometers and 200 micrometers, the susceptor being located within the aerosol forming substrate (20).
[0006]
6. An aerosol generating article according to claim 5, characterized in that the elongated susceptor is positioned in a radially central position within the aerosol-forming substrate and extends along the longitudinal axis of the aerosol-forming substrate.
[0007]
7. Aerosol generator article, according to any one of the preceding claims, characterized in that the second susceptor material is plated, deposited or welded to the first susceptor material.
[0008]
8. An aerosol generating article according to any one of the preceding claims, characterized in that the first susceptor material is in the form of an elongated strip having a width of between 3 mm and 6 mm and a thickness of between 10 microns. meters and 200 micrometers, the second susceptor material being in the form of discrete fragments that are plated, deposited or welded to the first susceptor material.
[0009]
9. An aerosol generating article according to any one of claims 1 to 7, characterized in that the first susceptor material and the second susceptor material are glued in the form of an elongated strip with a width of between 3 mm and 6 mm and a thickness of between 10 micrometers and 200 micrometers, the first susceptor material having a greater thickness than the second susceptor material.
[0010]
10. Aerosol generating article according to any one of claims 1 to 7, characterized in that the susceptor is an elongated susceptor with a width of between 3 mm and 6 mm and a thickness of between 10 micrometers and 200 micrometers, the susceptor comprising a core of the first susceptor material encapsulated by the second susceptor material.
[0011]
11. An aerosol generating article according to any one of the preceding claims, characterized in that the first susceptor material is for heating the aerosol forming substrate and the second susceptor material is for determining when the susceptor reaches a temperature corresponding to the temperature of Curie of the second susceptor material.
[0012]
12. An aerosol generating article according to any one of the preceding claims, characterized in that the aerosol-forming substrate is in the form of a column comprising a grouped sheet of aerosol-forming material, for example a grouped sheet of homogenized tobacco or a grouped sheet comprising a nicotine salt and an aerosol former.
[0013]
13. Aerosol generator article, according to any one of the preceding claims, characterized in that it comprises more than one susceptor (1,4).
[0014]
14. Aerosol generating system, characterized in that it comprises an electrically operated aerosol generating device (200) having an inductor (210) for producing a variable electromagnetic field and an aerosol generating article (10) as defined in any of the claims 1 to 12, the aerosol generating article (10) in engagement with the aerosol generating device (200) so that the variable magnetic field produced by the inductor (210) induces a current in the susceptor (1,4), causing that the susceptor (1,4) has its temperature increased, whereby the electrically operated aerosol generating device comprises electronic circuits configured to detect the Curie transition of the second susceptor material.
[0015]
15. Aerosol generating system according to claim 14, characterized in that the electronic circuits are adapted for a closed-loop control of the heating of the aerosol forming substrate.
[0016]
16. System according to claim 14 or 15, characterized in that the electrically operated aerosol generating device is capable of inducing a variable magnetic field with a frequency of between 1 and 30 MHz and a field strength H of between 1 and 5 kiloamps per meter (kA/m) and the susceptor in the aerosol generating article being capable of dissipating energy of between 1.5 and 8 Watts when positioned within the variable magnetic field.
[0017]
17. Method of using an aerosol generating article as defined in any one of claims 1 to 13, characterized in that it comprises the steps of positioning the article in relation to an electrically operated aerosol generating device so that the article susceptor being within a variable electromagnetic field generated by the device, the variable electromagnetic field causing the susceptor to be increased in temperature and monitoring at least one parameter of the electrically operated aerosol generating device to detect the Curie transition of the second susceptor material.
[0018]
18. Method according to claim 17, characterized in that the method further comprises controlling the electromagnetic field using electronic circuits so that the temperature of the susceptor is maintained at the Curie temperature of the second susceptor material plus or minus 20° Ç.

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法律状态:
2020-02-18| B06U| Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette]|

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2021-02-23| B06A| Patent application procedure suspended [chapter 6.1 patent gazette]|

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2021-06-08| B09A| Decision: intention to grant [chapter 9.1 patent gazette]|

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2021-08-03| B350| Update of information on the portal [chapter 15.35 patent gazette]|

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2021-08-24| B16A| Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]|Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 21/05/2015, OBSERVADAS AS CONDICOES LEGAIS. |

优先权:

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申请号 | 申请日 | 专利标题

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EP14169192.3|2014-05-21|

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EP14169241.8|2014-05-21|

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EP14169241|2014-05-21|

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EP14169192|2014-05-21|

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EP14169194.9|2014-05-21|

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EP14169194|2014-05-21|

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PCT/EP2015/061293|WO2015177294A1|2014-05-21|2015-05-21|Aerosol-generating article with multi-material susceptor|

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